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Michael A Eckhoff, 7016204 Stearns St, Overland Park, KS 66221

Known as:
Michael Eckhoff Ret Mike A Eckhoff Michael Eckhoss Michael F
Related to:
Scott M Lewis 66

Michael Eckhoff Phones & Addresses

8 Clyde St, Somerville, MA 02145   

Ridgefield, CT   

12130 Melrose St, Overland Park, KS 66213    913-8976613   

Shawnee Mission, KS   

Cincinnati, OH   

Danbury, CT   

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Michael Eckhoff Photo 32

Michael Eckhoff

Location:
United States

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Us Patents

Synthesis Of Alpha-Tocopherolquinone Derivatives, And Methods Of Using The Same

US Patent:
2011026, Oct 27, 2011
Filed:
Mar 9, 2011
Appl. No.:
13/044056
Inventors:
Steven D. PAISLEY - Danbury CT, US
Jason M. LePree - Demarest NJ, US
Amale Hawi - Ridgefield CT, US
Michael Eckhoff - Ridgefield CT, US
Assignee:
Penwest Pharmaceuticals Co. - Patterson NY
International Classification:
A61K 31/122
C07C 49/497
A61P 25/00
A61P 3/10
A61P 25/28
A61P 25/18
A61P 35/00
C07C 45/60
A61P 25/08
US Classification:
514678, 568323, 568308
Abstract:
The present invention is directed to a method of synthesizing a compound of Formula I:the method comprising oxidizing alpha-tocopherol with a metal salt oxidizing agent to form the compound of Formula I, wherein the stoichiometric ratio (mol/mol) of metal salt oxidizing agent/alpha-tocopherol is 1.6 to 4. The invention is also directed to a method of synthesizing a compound of Formula I, the method comprising (a) hydrolyzing alpha-tocopheryl acetate in the presence of a base; (b) neutralizing the hydrolyzing of (a), thereby forming alpha-tocopherol; and (c) oxidizing the alpha-tocopherol of (b) with a metal salt oxidizing agent to form the compound of Formula I, wherein the stoichiometric ratio (mol/mol) of metal salt oxidizing agent/alpha-tocopherol is 1.6 to 4.

Possible Relatives

Deborah M Eckhoff  Daniel Eckhoff  Denise M Eckhoff  Danny C Eckhoff  Diane P Eckhoff  Dolores H Eckhoff  Donald R Eckhoff  Michael C Last  Michael C Johnson  Michael F Stamps 

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